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Purification process for partly-hydrolyzed cellulose
专利权人:
James M. Lockhart
发明人:
James M. Lockhart
申请号:
US14422619
公开号:
US09567707B2
申请日:
2012.08.21
申请国别(地区):
US
年份:
2017
代理人:
摘要:
A method of recovering purified partly-hydrolyzed cellulose (36) from a composition (14) comprising partly-hydrolyzed cellulose and an acid, such as sulfuric acid. A base (28) having a cation that forms a precipitate with the anion of the acid is added to the composition. For example, a base such as barium hydroxide is added to form a sulfate precipitate. The precipitate (38) is then separated from the partly-hydrolyzed cellulose (36), thus reducing its acid content. The method may include additional steps of centrifugation (18) of the composition, breaking-up agglomerations (44) in the composition after precipitation, and dialysis (42).
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