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(E)-oxime of 4-ethyl-4'-phenylchalcone and (Z)-oxime of 4-ethyl-4'-phenylchalcone and method for obtaining them simultaneously
专利权人:
UNIWERSYTET PRZYRODNICZY WE WROCŁAWIU
发明人:
BARTŁOMIEJ POTANIEC,MIROSŁAW ANIOŁ
申请号:
PL424475
公开号:
PL234094B1
申请日:
2018.02.02
申请国别(地区):
PL
年份:
2020
代理人:
摘要:
The scope of the notification is the compound (E)-4 -ethyl -4'-phenylchalcone oxide with formula 2 and (Z)-4 -ethyl -4'-phenylchalcone oxide with formula 3. The notification shall also include the means of receiving them simultaneously. This means that a hydroxylamine hydrochloride, anhydrous sodium sulphate (VI), a mixture of organic solvents and the apparatus are added to the substrate, which is 4 -ethyl -4'-phenylchalkon of model 1. After dissolving the substrates, pyridine is added,which is a reaction mixture,which is protected from light and kept at a temperature from 18oC to 28oC for a period of five to 14 days. The reaction mixture is poured into cold water or ice water and then extracted with an organic solvent that does not mix with water,dry with anhydrous magnesium sulphate and /or anhydrous sodium sulphate and the solvent evaporates,the extract obtained is then purified on a chromatographic column.
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