The present invention relates to feed for a goat containing sulfur and a manufacturing method thereof. A manufacturing method thereof comprises: a powder sulfur and persimmon vinegar preparation process (S10) of preparing powered sulfur and liquid persimmon vinegar; a powder sulfur and persimmon vinegar mixing process (S20) of putting and mixing 50 wt% of the liquid persimmon vinegar with respect to the weight of the powdered sulfur in a container; a sulfur and persimmon vinegar mixture heating process (S30) of heating a mixture of the sulfur and the persimmon vinegar for 50 to 60 minutes to make the temperature of the mixture of the sulfur and the persimmon vinegar reach 100 to 120°;C; a sulfur and persimmon vinegar mixture cooling and coagulating process (S40) of pouring the heated sulfur and persimmon vinegar mixture in the liquid persimmon vinegar contained in an additional container, naturally cooling the mixture for 60 to 90 minutes at room temperature, and coagulating the mixture; a coagulated sulfur and persimmon vinegar mixture grinding process (S50) of grinding the coagulated sulfur and persimmon vinegar mixture into a powder state using a grinder; a repetition process (S60) of mixing the mixture with 50 wt% of the persimmon vinegar with respect to the sulfur and persimmon vinegar mixture powder gained from the mixture grinding process (S50), and repeating a process from the second step (S20) to the fifth step (S50) eight times; and a feed mixing process (S70) of mixing 300 to 400 wt% of general feed for a goat with respect to the weight of the ground sulfur and persimmon vinegar mixture which is gained through nine times of repetition including the repetition process (S60).본 발명은 유황이 함유된 염소사료 및 그 제조방법에 관한 것으로서, 그 구체적인 공정은, 분말 상태의 유황과 액상의 감식초를 준비하는 분말 유황 및 감식초 준비공정(S10)과, 상기 분말 유황의 무게에 대하여 50중량%에 해당하는 액상의 감식초를 유황과 함께 용기에 넣고 혼합하는 분말 유황과 감식초 혼합공정(S20)과, 유황과 감식초의 혼합물의 온도가 100~120℃에 이르도록 50~60분 동안 가열하는 유황과 감식초의 혼합물 가열공정(S30)과, 가열된 유황과 감식초의 혼합물을 별도의 용기에 담겨진 액