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PREPARATION METHOD FOR MEDICAL POROUS TANTALUM IMPLANT MATERIAL
专利权人:
CHONGQING RUNZE PHARMACEUTICAL COMPANY LIMITED.
发明人:
YE, Lei,叶雷
申请号:
CNCN2012/082225
公开号:
WO2013/044833A1
申请日:
2012.09.27
申请国别(地区):
WO
年份:
2013
代理人:
摘要:
A preparation method for a medical porous tantalum material comprising mixing tantalum powder and an aqueous solution of polyglycolic into a slurry, injecting the slurry into an organic foamed body by using pressuring by vibration, then drying, degreasing, sintering, cooling, and performing a heating process the mass concentration of the aqueous solution of polyglycolic is 2% to 8%, and the vibration frequency is 20 to 80 times/minute the sintering step comprises: within a vacuum degree of 10-4 to 10-3 Pa, increasing the temperature to 1500 to 1800°C at a speed of 10 to 20°C/min, maintaining the temperature for 120 to 240 minutes, cooling together with the furnace to 200 to 300°C, increasing the temperature to 1500 to 1800°C at a speed of 10 to 20°C/min, maintaining the temperature for 180 to 240 minutes, increasing the temperature to 2000 to 2200°C at a speed of 5 to 10°C/min, and maintaining the temperature for 120 to 360 minutes the heating process step comprises: within a vacuum degree of 10-4 to 10-3 Pa, increasing the temperature to 800 to 900°C at a speed of 10 to 20°C/min, maintaining the temperature for 240 to 480 minutes, cooling to 400°C at a speed of 2 to 5°C/min, maintaining the temperature for 120 to 300 minutes, and cooling together with the furnace to room temperature. The porous tantalum prepared using the present method is suitable as a medical implant material for weight-bearing bone tissue replacement, and ensures both biocompatibility and mechanic properties.Procédé de préparation dun matériau au tantale poreux à usagemédical, selon lequel une solution aqueuse dalcool polyvinlyique est liée à une suspension de poudre de tantale, la suspension étant ajoutée moyennant pression vibratoire à un corps mousseux organique et le mélange étant, par la suite, soumis à séchage, décrassage, frittage, refroidissement et chauffage afin dobtenir un matériau de tantale poreux à usage médical. Ce matériau au tantale poreux de substitution dun tissu osseux de sup
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