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METHOD AND DEVICE FOR PROCESSING WASTE SULPHURIC ACIDS FROM NITRATION PROCESSES
专利权人:
De Dietrich Process Systems GmbH
发明人:
Dichtl, Gottfried,Steeg, Harald
申请号:
HUE09011773
公开号:
HUE029763(T2)
申请日:
2009.09.15
申请国别(地区):
匈牙利
年份:
2017
代理人:
摘要:
Processing waste acid obtained from nitroaromatics production, preferably dinitrotoluene- or trinitrotoluene production, comprises: adding a pre-heated waste acid comprising sulfuric acid, water, nitric acid, nitrosylsulfuric acid and nitro-organics, into a stripping column in a counter-flow to the steam obtained from the bottom of the stripping column by heating a pre-concentrated sulfuric acid; separating nitric acid, optionally nitro-organics and the pre-concentrated sulfuric acid into at least one vapor phase; and processing the obtained nitric acid and the nitro-organics. Processing waste acid obtained from nitroaromatics production, preferably dinitrotoluene- or trinitrotoluene production, under recovery of concentrated and purified sulfuric acid and nitric acid, comprises: (i) adding a pre-heated waste acid comprising sulfuric acid and water (up to 80 wt.%), nitric acid, nitrosylsulfuric acid and nitro-organics, preferably dinitrotoluene and mononitrotoluene, into a stripping column in a counter-flow t
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