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PROCESS FOR PRODUCTION OF A POLYMORPH OF 2-(3-CYANO-4- ISOBUTYLOXYPHENYL)-4-METHYL-5-THIAZOLECARBOXYLIC ACID
专利权人:
发明人:
申请号:
EP07767403.4
公开号:
EP2039691B1
申请日:
2007.06.22
申请国别(地区):
EP
年份:
2013
代理人:
摘要:
A method for producing crystal A of 2-(3-cyano-4-isobutyloxyphenyl)-4-methyl-5-thiazolecarboxylic acid by dissolving 2-(3-cyano-4-isobutyloxyphenyl)-4-methyl-5-thiazolecarboxylic acid in methanol or a mixed solvent of methanol and water (the volume ratio of methanol to water is 90/10 or more), then adding water until the ratio of methanol to water becomes 7/3, and further adding a specific amount of a seed crystal at a specific timing during the addition of water.
来源网站:
中国工程科技知识中心
来源网址:
http://www.ckcest.cn/home/

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