Markus Henrich,Simona Negura,Gergely Tasi,Pal Kocsan,Federico Sbrogio,Michael Pyerin,Herbert Koller
申请号:
US13138883
公开号:
US08784847B2
申请日:
2010.04.16
申请国别(地区):
US
年份:
2014
代理人:
摘要:
Process for manufacturing 1-amino-1,3,3,5,5-pentamethylcyclohexane mesylate comprising step (i):(i) reacting 1-amino-1,3,3,5,5-pentamethylcyclohexane with methane sulfonic acid in a solvent or a mixture of two or more solvents selected from anisole, cumene, pentane, hexane, heptane, isooctane, methyl acetate, propyl acetate, isopropyl acetate, n-butyl acetate, isobutyl acetate, methyl ethyl ketone, methyl isopropylketone, methyl isobutyl ketone, dimethyl sulphoxide, tetrahydrofuran, methyltetrahydrofuran, 1,1-diethoxypropane, 1,1-dimethoxymethane, and 2,2-dimethoxypropane.