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PROCESS AND DEVICE FOR PRODUCING NANOGELS AND MICROGELS BASED ON ALKALINE EARTH SILICATES
专利权人:
JUMANCA DANIELA
发明人:
JUMANCA DANIELA,JUMANCA DANIELA,GĂLUŞCAN ATENA,GĂLUŞCAN ATENA,BORCAN FLORIN,BORCAN FLORIN,FLORIŢA ŞERBAN,FLORIŢA ŞERBAN,DEHELEAN CRISTINA,DEHELEAN CRISTINA,FLORIŢA ZENO,FLORIŢA ZENO
申请号:
RO201200528
公开号:
RO128480B1
申请日:
2012.07.13
申请国别(地区):
RO
年份:
2016
代理人:
摘要:
The invention relates to a process for preparing alkaline earth silicates applied in medical dentistry and to an installation for applying the process. The claimed process consists in the chemical reaction at temperatures of 20...50°C of magnesium, calcium or barium salt or hydrosoluble, partially soluble or insoluble hydroxide, in phase emulsion made with a jet of carrier gas or liquid in uniflow, at a pressure of 1.2...3 bar, with lithium, sodium or potassium alkaline silicate, the reactant solution having concentrations of 1...20% by weight, in a reaction area with internal partial recirculation of the emulsion, the resulting silicate hydrogel is separated by ultra-centrifuging, possibly filtered under vacuum, followed by repeated washing with distilled water, the paste resulting from separation being conditioned by drying, wherefrom there results a solid powder having a grain size of 100...1000 nm. The claimed installation comprises a chemical reactor () provided with two static mixers (), a connection () for injecting the carrier gas, two connections () for injecting the aqueous solutions, two dosing vessels (), two heat exchangers () for preheating the aqueous solution, a vertical cylindrical vessel () for separating the emulsion hydrogel and a column () for separating the gas/liquid drops and exhausting the residual gas.Invenţia se referă la un procedeu pentru obţinerea unor silicaţi alcalino-pământoşi, cu aplicaţie în domeniul medicinei dentare, şi la o instalaţie pentru aplicarea procedeului. Procedeul conform invenţiei constă din reacţia chimică, la temperaturi de 20...50°C, a unei sări sau hidroxid hidrosolubil, parţial solubil sau insolubil în apă, de magneziu, calciu sau bariu, în fază emulsionată cu un jet de gaz portant/lichid în echicurent, la o presiune de 1,2...3 bar, cu un silicat alcalin de litiu, sodiu sau potasiu, soluţiile reactante având concentraţii de 1...20% în greutate, într-o zonă de reacţie cu recircularea internă parţială a emulsiei, h
来源网站:
中国工程科技知识中心
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