SYVRET ROBERT G,POLSZ CRAIG A,SWAN DANA L,SRINIVAS VIJAY R
申请号：
IN201717003097
公开号：
IN201717003097A
申请日:
2017.01.27
申请国别(地区):
IN
年份:
2017
代理人:
摘要：
A method of making CF3CH2SH comprising a step of reacting CF3CH2X wherein X is halide or tosylate with MSH where M is an alkali metal such as Na or K to yield CF3CH2SH. More specifically a method of making CF3CH2SH a step of reacting CF3CH2CI with a molar excess of NaSH in a reaction medium of one or more polar organic solvents at a temperature of from about 70C to about 110C for a time of from about 1 to about 5 hours.
