Extraction Procedure of unsaponifiable fraction contained in oil or Shortening from microorganism comprising stage of transformation of such Oils, alcoholic solvent extraction with at least 5 Carbon Atoms or one or two Oxygen Atoms INSAP fraction; Onificable; and use of HMDS.
The present invention relates to an extraction process of an unsaponifiable fraction contained in an oil or a vegetable butter, in an oil originating from a micro-organism, in a concentrate of oil or butter or of oil originating from a micro-organism, or in a co-product of the refining industry for vegetable oils, such as deodorisation exhaust and distillates of physical refining, or oils originating from micro-organisms, comprising at least: A) a transformation step of said oils, of said butter or said co-product of the refining industry for vegetable oils or oils originating from micro-organisms in hydro-alcoholic solution, especially via a saponification step, and B) an extraction step of the hydro-alcoholic solution in which the fatty fraction is separated from unsaponifiable fraction by liquid/liquid extraction, said process being characterised in that at least the liquid/liquid extraction step of the step B is performed by using a first solvent system comprising a solvent content selected from the solvents comprising at least 5 carbon atoms and one or two oxygen atoms in the form of either ether function, or ketone function, or ester function, of at least 50% in volume relative to the total volume of the first solvent system, as well as fractions obtained by said process.Procedimiento de extracción de una fracción insaponificable contenida en un aceite o una manteca vegetal, en un aceite que procede de un microorganismo, en un concentrado de aceite o de manteca vegetal o de aceite que procede de un microorganismo, o en un co-producto de la industria del refinado de los aceites vegetales, tales como las fugas de desodorizacion y los destilados de refinado físico, o de los aceites que proceden de microorganismos, que comprende una etapa de transformación de dicha materia grasa en solución hidroalcohólica, a través de una etapa de saponificación, y una etapa de extracción de la solución hidroalcohólica en la que la fracción grasa se separa de la fracción insaponi