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シラン変性カチオン化セルロースの製造方法
专利权人:
ライオン株式会社
发明人:
河野 洋一郎,大迫 陽子,伊藤 篤司
申请号:
JP2009529072
公开号:
JP5298018B2
申请日:
2008.08.22
申请国别(地区):
JP
年份:
2013
代理人:
摘要:
A method of producing silane-modified cationized cellulose that has excellent aqueous dispersibility, including: a step (1) of cationizing water-soluble cellulose ether in a presence of alkali in a mixed solvent of a water-compatible organic solvent and water to obtain slurry comprising cationized cellulose a step (2) of adding acid to said slurry and neutralizing said alkali a step (3) of reacting said cationized cellulose obtained after said neutralization with an amino silane compound which is 0.3-10% by mass relative to an amount of water-soluble cellulose ether used in step (1) and a step (4) of drying the obtained slurry, wherein: drying is conducted in step (4) at 115-160°C until weight loss on drying is 5% by weight or less, or there is also including a step (5) of adding a water-compatible organic solvent or a mixed solvent of a water-compatible organic solvent and water to the cationized cellulose after the neutralization so that water content in a whole solvent that contacts the cationized cellulose is 10% by mass or less.
来源网站:
中国工程科技知识中心
来源网址:
http://www.ckcest.cn/home/

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