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PROCESS FOR PREPARING 2-EXO-(2-METHYLBENZYLOXY)-1-METHYL-4-ISOPROPYL-7-OXABICYCLO[2.2.1]HEPTANE
专利权人:
BASF AGRO B.V.
发明人:
BENSON, Stefan,RACK, Michael,ALZNAUER, Christiane,GOETZ, Roland,WOLF, Bernd
申请号:
WO2018EP57397
公开号:
WO2018177907(A1)
申请日:
2018.03.23
申请国别(地区):
世界知识产权组织国际局
年份:
2018
代理人:
摘要:
This invention relates to a process for preparing (±)-2-exo-(2-Methylbenzyloxy)-1-methyl-4-isopropyl-7-oxabicyclo[2.2.1]heptane of the formula (I) (I), any of its individual enantiomers or any non-racemic mixture thereof, comprising the step of reacting (±)-2-exo-hydroxy-1-methyl-4-isopropyl-7-oxabicyclo[2.2.1]heptane of the formula (II) (II), any of its individual enantiomers or any non-racemic mixture thereof with a 2-Methylbenzyl compound of the formula (III) (III), wherein X is a leaving group, in the presence of at least one base, at least one catalyst selected from rubidium salts, cesium salts and any combination thereof and at least one inert organic solvent S1.
来源网站:
中国工程科技知识中心
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