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PRODUCTION METHOD OF WATER-INSOLUBLE AROMATIC COMPOUND INCLUDING COMPOSITION
专利权人:
KAO CORP;花王株式会社
发明人:
SUZUKI TAKASHI,鈴木 高,ABE TETSUYA,阿部 哲也,TAKAHASHI RUI,高橋 塁,ENDO KOJI,遠藤 浩二,TSUCHIKURA TOYOKI,土倉 豊樹,IWAI HIDETAKA,岩井 秀隆,HORIZUMI TERUO,堀住 輝男,AOSAKI TAISUKE,青崎 泰輔,UDA AKIHIRO,宇田 晶宏,NAKAMICHI MASA
申请号:
JP2018246292
公开号:
JP2019119740A
申请日:
2018.12.27
申请国别(地区):
JP
年份:
2019
代理人:
摘要:
To provide a novel method for producing a water-insoluble aromatic compound including composition excellent in solubility of a water-insoluble aromatic compound.SOLUTION: The method comprises: a step (1) for acquiring a water-insoluble aromatic compound solution 1 including a step (1-1) for preparing a heating processing raw material including (A) water-insoluble aromatic compound, (B) polyol, (C) aqueous medium, and a step (1-2) for heating processing the heating processing raw material at temperature less than 100°C at normal pressure for acquiring a water-insoluble aromatic compound including heating processing liquid; and a step (2) for adding water to the water-insoluble aromatic compound solution 1 for acquiring a water-insoluble aromatic compound solution 2 in which a density of the (A) water-insoluble aromatic compound becomes a density exceeding saturation solubility at 25°C. In the step (1), a content of a surfactant in the heating processing raw material is 0.1 mass% or less, and a content of the (A) water-insoluble aromatic compound in the heating processing raw material is less than saturation solubility at 25°C with respect to a solvent of a same composition of the (A) water-insoluble aromatic compound.SELECTED DRAWING: None【課題】難水溶性芳香族化合物の溶解性に優れる難水溶性芳香族化合物含有組成物を製造する新たな方法の提供。【解決手段】 (A)難水溶性芳香族化合物、(B)ポリオール及び(C)水性媒体を含有する加熱処理原料を調製する工程(1-1)と、前記加熱処理原料を常圧で100℃未満の温度で加熱処理して、難水溶性芳香族化合物含有加熱処理液を得る工程(1-2)とを含む、難水溶性芳香族化合物溶液1を得る工程(1)と;前記難水溶性芳香族化合物溶液1に水を加えて、(A)難水溶性芳香族化合物が25℃における飽和溶解度超の濃度となる難水溶性芳香族化合物溶液2を得る工程(2)とを含み、 前記工程(1)において、加熱処理原料中の界面活性剤の含有量が0.1質量%以下であり、かつ加熱処理原料中の(A)難水溶性芳香族化合物の含有量が、(A)難水溶性芳香族化合物の同一組成の溶媒に対する25℃における飽和溶解度未満である、難水溶性芳香族化合物含有組成物の製造方法。【選択図】なし
来源网站:
中国工程科技知识中心
来源网址:
http://www.ckcest.cn/home/

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