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(E)-oxime of 4'-phenyl-4-carboxychalcone and (Z)-oxime of 4'-phenyl-4-carboxychalcone and method for obtaining them simultaneously
专利权人:
UNIWERSYTET PRZYRODNICZY WE WROCŁAWIU
发明人:
BARTŁOMIEJ POTANIEC,MIROSŁAW ANIOŁ
申请号:
PL424476
公开号:
PL234095B1
申请日:
2018.02.02
申请国别(地区):
PL
年份:
2020
代理人:
摘要:
The scope of the notification is compounds (E)-4'-phenyl -4 -carboxyalkone, model 2, and (Z)-4'-phenyl -4 -carboxyalkone, model 3. The notification shall also cover the way in which they are received simultaneously. This means that the substrate, which is 4'-phenyl -4 -carboxycyclone of model 1, is supplemented with hydroxylamine hydrochloride, sodium sulphate (VI) anhydrous, followed by a mixture of organic solvents and the apparatus is filled with nitrogen. After dissolving the substrates, pyridine is added,which is a reaction mixture,which is protected from light and kept at a temperature from 18oC to 28oC for a period of five to 14 days. The reaction mixture is poured into cold water or ice water and then extracted with an organic solvent that does not mix with water,whose inputs are connected to the current sensor (CP) and the voltage sensor (CN). The Electricity Regulatory System (URP) is equipped with a sumer whose output is the output of the Electricity Regulatory System (URP) and the first input of the sumer is connected to the regulator, the second input of the sumer is connected to the processing block (BP) by means of a top -pass filter and the third input of the sumer is connected to the voltage sensor (CN). Mode of operation of voltage transducer (PE) connected to the power grid (SNP) via a network filter (F),where the output voltage of the transformer is determined by means of a power regulation system (URP),
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