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MANUFACTURE OF CRYSTALLITE PARTICLES
专利权人:
Magnus Odén;Emma Björk
发明人:
Magnus Odén,Emma Björk
申请号:
US13825454
公开号:
US20140030180A1
申请日:
2011.09.21
申请国别(地区):
US
年份:
2014
代理人:
摘要:
A method for the manufacture of crystallite particles, said method comprising the steps of: a) reacting a reaction solution comprising a silicate, a micelle forming agent, an alkane, a salt under stirring at pH 2 or lower, wherein the reaction solution comprises HCI in a concentration of at least 1.5 M, wherein the stirring is performed not more than 10 minutes, and b) treating the obtained material to remove the micelle forming agent with one method selected from i) heat treating the material above 300° C., ii) treating the material with at least one selected from H2O2, and H2SO4, iii) treating the material with microwaves to digest the micelle forming agent. An advantage is that the time for the synthesis is shortened considerably compared to the prior art.
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