1. crystal compound of formula ii.where the sol is a solventm equals 0.1 ~ 2, preferably 0.5 ~ 1.5, more preferably 1.2. crystal for p.1, where the solvent chosen from the group consisting of ether such as diethyl ether, diisopropyl ether, tetrahydrofuran and \u0434\u0438\u043c\u0435\u0442\u043e\u043a\u0441\u0438\u044d\u0442\u0430\u043d, \u043f\u0440\u0435\u0434\u043f\u043e\u0447\u0442\u0438\u0442\u0435\u043b\u044c\u043d the diethyl ether, diisopropyl ether, ester, such as \u043c\u0435\u0442\u0438\u043b\u0430\u0446\u0435\u0442\u0430\u0442, ethyl acetate and ethyl formate, preferably ethyl acetate, ketones such as acetone, and boo \u0442\u0430\u043d\u043e\u043d, preferably acetone nitrilessuch as acetonitrile and \u043f\u0440\u043e\u043f\u0438\u043e\u043d\u0438\u0442\u0440\u0438\u043b, preferably acetonitrile \u0434\u0438\u043f\u043e\u043b\u044f\u0440\u043d\u044b\u0435 aprotic solvents, such as \u0434\u043c\u0444\u0430 and dhs, preferably dhs acid ra \u0442\u0432\u043e\u0440\u0438\u0442\u0435\u043b\u0438, such as formic acid and acetic acid, preferably acetic acid, and water.3. crystal compound of formula ii.where the sol is an acetic acidm equals 1.4. crystal for x-ray crystal powder 3 is measured in the light of cu K\u03b1, diffracted peaks, expressed as \u043c\u0435\u0436\u043f\u043b\u043e\u0441\u043a\u043e\u0441\u0442\u043d\u043e\u0433\u043e distance d,re locat 10,43 \/ are brought about in \u01fa, 8,63 \u01fa, 7.20 \u01fa, 6.33 \u01fa, 5.15 \u01fa and 3.47 \u01fa.5. crystal on paragraph 4, where powdered crystal x-ray radiation measured in cu K\u03b1, diffracted peaks, expressed as \u043c\u0435\u0436\u043f\u043b\u043e\u0441\u043a\u043e\u0441\u0442\u043d\u043e\u0433\u043e distance d,re locat 10,43 \/ are brought about in \u01fa, 8,63 \u01fa, 7.20 \u01fa, 6.33 \u01fa, 5.15 \u01fa, 4.80 \u01fa, male \u01fa, 3,77 \u01fa, 3.68 \u01fa and 3.47 \u01fa.6. the on clause 5 in which crystal powder x-ray radiation measured in cu K\u03b1, diffracted peaks, expressed as \u043
