PROBLEM TO BE SOLVED: To provide powdery or encapsulated compositions containing fat-soluble materials to be blended into food products, beverages, animal feeds, cosmetics or pharmaceuticals as additives.SOLUTION: There is provided a preparation method of a composition comprising a) a matrix material forming an outer continuous phase and b) an inner discontinuous phase within the matrix material, the inner discontinuous phase comprising: a fat-soluble physiologically active component; and a physiologically acceptable encapsulating material which is solid at a room temperature and which is homogeneously soluble in an organic solvent together with the fat-soluble physiologically active component. The composition comprises, as the encapsulating material, wax or wax-like material, or beeswax or carnauba wax, and as the matrix material, gelatin, lignosulfonate, milk protein or hydrolyzed milk protein, plant protein or hydrolyzed plant protein, or modified starch. The composition comprises, as the fat-soluble physiologically active material component, alkaloid such as astaxanthin or canthaxanthin, or polyunsaturated fatty acid.【課題】食品、飲料、動物飼料、化粧品又は薬品に添加物として混合する脂溶性物質を含む、粉状又はカプセル化組成物の提供。【解決手段】a)外部連続相を形成するマトリックス物質、及び、b)脂溶性生理活性成分と、室温で固体であり、該脂溶性生理活性成分とともに有機溶媒に均質に可溶である、生理学的に許容可能なカプセル化物質、を含む前記マトリックス物質内の内部不連続相を含む組成物の調製方法。前記カプセル化物質は、ワックス又はワックス様物質若しくは、ミツロウ又はカルナウバロウ;前記マトリックス物質は、ゼラチン、リグノスルホネート、牛乳タンパク又は加水分解牛乳タンパク、植物タンパク質又は加水分解植物タンパク質若しくは改変デンプンを含む組成物。前記脂溶性生理活性物質成分がアスタキサンチン又はカンタキサンチン等のアルカイド若しくは、多不飽和脂肪酸である組成物。【選択図】なし