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Probehead of an NMR-MAS apparatus with a device for determining the angle between the MAS rotor and the static magnetic field
专利权人:
Bruker BioSpin AG
发明人:
Freytag Nicolas
申请号:
US201715441991
公开号:
US9945654(B2)
申请日:
2017.02.24
申请国别(地区):
美国
年份:
2018
代理人:
Edell, Shapiro & Finnan, LLC
摘要:
A probehead of an NMR-MAS apparatus with a rotation axis (RA), which lies in an xz-plane, titled by an angle θ>0 relative to a z-axis. The angle θ is adjusted by tilting around a tilt axis (DA) parallel to the y-axis relative to a target angle θtarget. An angle measurement apparatus (9) has a first sensor element (7), which, together with a second sensor element (8) generates sensor signals dependent on the amplitude B0 of the static magnetic field and the vectorial orientation between the magnetic field B0 and a sensitivity vector. Two sensitivity vectors have an angle 5°<αi<175° to the z-axis and an angle β>10° to each other. The angle between the rotation axis and the z-axis can be measured precisely and reliably over a large range, providing a feedback signal for regulated adjustment or tracking of the angle θ.
来源网站:
中国工程科技知识中心
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