Vlaamse Instelling Voor Technologisch Onderzoek (VITO)
发明人:
Steven Mullens,Ivo Thijs,Jozef Cooymans,Jan Luyten
申请号:
US14667403
公开号:
US09464342B2
申请日:
2015.03.24
申请国别(地区):
US
年份:
2016
代理人:
摘要:
A method for manufacturing a high ductility Ti-, Ti-alloy or NiTi-foam, meaning a compression strain higher than 10%, includes: preparing a powder suspension of a Ti-, NiTi- or Ti-alloy powder, bringing the said powder suspension into a desired form by gelcasting to form a green artifact. The method also includes a calcination step wherein the green artifact is calcined, and sintering the artifact. The calcination step includes a slow heating step wherein said green artifact is heated at a rate lower or equal to 20° C./hour to a temperature between 400° C. and 600° C. and the Ti-, NiTi- or Ti-alloy powder has a particle size less than 100 μm. A high ductility Ti-, Ti-alloy or NiTi foam, with a compression higher than 10%, with a theoretical density less than 30%, pore size (cell size) between 50 to 1000 μm can be obtained with such a method.