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PROCÉDÉ DE PRODUCTION D'UN IMPLANT ORTHOPÉDIQUE PERSONNALISÉ, BIOCOMPATIBLE ET BIOACTIF
专利权人:
Nano-implant Sp. z o.o.
发明人:
申请号:
EP18020636.9
公开号:
EP3666932A1
申请日:
2018.12.14
申请国别(地区):
EP
年份:
2020
代理人:
摘要:
The production method of the implant made of Ti6A14V titanium alloy with a coating made of titanium dioxide nanotubes includes the creation of a virtual implant model on the basis of computer tomography images of the anatomical shape of the bone from before a fracture and the adjustment of the shape of the implant to the anatomical shape of the bone, and then creation in the process of selective laser sintering of Ti6A14V titanium alloy powder in 3D printing technology, and then a thermal stress relieving and mechanical preparation of the surface by a sandblasting method. Thereafter, the surface is degreased favourably in ethyl alcohol with the use of an ultrasonic cleaner and washed in distilled water also with the use of an ultrasonic cleaner, then the implant is immersed for 20-40 seconds in a mix of the hydrofluoric acid pure for analysis (p.a.), nitric acid (V) (p.a.) and distilled water, mixed in a 1:4:5 to 2:3:6 ratio. Then, a process of anodic oxidation of the implant surface is carried out in 0.3% solution of the hydrofluoric acid (p.a.) for 15-25 minutes, at a voltage of 5 V to 8V with the implant as an anode with a distance of 1.5 to 2.5 cm between a platinum plate as a cathode. After the anodic oxidation process, the implant is washed in distilled water by means of an ultrasonic cleaner with the addition of Al2O3 powder whose grain sizes are equal to 50 nm and then it is washed in acetone (p.a.) also with the use of an ultrasonic cleaner and dried in an argon beam and then it is held in a dryer at a temperature of 393 K. Titanium dioxide nanotubes of 100-150 nm thick and nanotube diameter of 18 to 25 nm are created on the surface of the implant.
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中国工程科技知识中心
来源网址:
http://www.ckcest.cn/home/

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