The present invention relates to novel and useful pharmaceutical compositions formulated with a cyclodextrin compound and a budesonide derivative for the treatment and/or prevention of pulmonary inflammatory disease. The present invention also relates to a novel and useful analytical technique for the detection and the quantification of HP-β-CD in solution. More specifically, the present invention relates to the use of a validated 1H NMR analysis for the detection and quantification of cyclodextrins directly in pharmaceutical formulations without any extraction or separation steps for liquid formulations.本發明係涉及新穎的和有用的醫藥組合物,其係以環糊精化合物和布地奈德衍生物配製,用於治療和/或預防肺部發炎性疾病。本發明也涉及新穎的和有用的分析技術,用於檢測和定量溶液中的HP-β-CD。尤其本發明涉及驗證過的1H NMR分析的使用,直接在液體醫藥製劑中檢測和定量環糊精,而不需任何的萃取或分離的步驟。