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Method for obtaining 7-methoxy-1,2,3-tris(4-methoxyphenyl)-1,2,3,4-tetrahydronaphthalene
专利权人:
POLITECHNIKA WARSZAWSKA
发明人:
HANNA KRAWCZYK,MARCIN POTERAŁA,PIOTR TOBIASZ
申请号:
PL424245
公开号:
PL233977B1
申请日:
2018.01.10
申请国别(地区):
PL
年份:
2019
代理人:
摘要:
The purpose of the notification is to obtain 7 -methoxy -1,2,3 -tris (4 -methoxyphenyl)-1,2,3,4 -tetrahydronaphthalene of model 1. That way is,that (E)-4,4'-dimethoxysilben is dissolved in methylene chloride,iodine 1 -1 mol /mol is added in relation to stilben and mixed for at least 20 -hour temperatures 20 -30,water is then added to the reaction mixture and extracted several times and the combined organic phases are washed with an aqueous solution of sodium pyrosircine,and then with water, the organic layer is dried with anhydrous MgSO4 and weighed.
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