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Process for recovering an esterified cellulose ether from a reaction product mixture
专利权人:
发明人:
Oliver Petermann,Matthias Sprehe,Robert Appell,Robert Nilsson
申请号:
US15022418
公开号:
US09587037B2
申请日:
2014.09.15
申请国别(地区):
US
年份:
2017
代理人:
摘要:
A process for recovering an esterified cellulose ether from a reaction product mixture obtained from a reaction of (a) a cellulose ether with (b) an aliphatic monocarboxylic acid anhydride or a di- or tricarboxylic acid anhydride or a combination of an aliphatic monocarboxylic acid anhydride and a di- or tricarboxylic acid anhydride, comprises the steps of (i) contacting the reaction product mixture with an aqueous liquid to precipitate the esterified cellulose ether from the reaction product mixture, (ii) isolating the precipitated esterified cellulose ether from the mixture obtained in step (i), and (iii) suspending the isolated esterified cellulose ether in an aqueous liquid to provide a suspension having a temperature of at least 28° C., and (iv) recovering the esterified cellulose ether from the suspension of step (iii).
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