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LIQUID/LIQUID EXTRACTION
专利权人:
라보라토이레즈 익스펜사이언스;LABORATOIRES EXPANSCIENCE
发明人:
SAUNOIS ALEX,소냐, 알렉,LEGRAND JACQUES,르그랑, 쟉끄,MERCIER EGLANTINE,므르씨에르, 에글랑뗑
申请号:
KR1020127020242
公开号:
KR1020120139690A
申请日:
2011.01.31
申请国别(地区):
KR
年份:
2012
代理人:
摘要:
The invention relates to a method for the extraction of all unsaponifiable fraction contained in a vegetable oil, an oil originating from a micro-organism or a vegetable butter or in a co-product from the vegetable oil refining industry, such as deodorization discharge. The method includes at least: A) a step comprising the transformation of the aforementioned oils, butter or co-product from the vegetable oil refining industry or oils originating from micro-organisms into a hydro-alcoholic solution by means of, in particular, a step selected from saponification and esterification steps; B) a step comprising the extraction of the hydro-alcoholic solution in which the fatty fraction is separated from the unsaponifiable fraction by means of liquid/liquid extraction; and C) an optional step comprising the purification of the unsaponifiable fraction, selected from the group containing crystallization and liquid/liquid extraction steps. According to the invention, at least one step from the liquid/liquid extraction steps in step B, the crystallization steps in step C and the liquid/liquid extraction steps in step C is performed using a first solvent system containing a concentration of solvent selected from among: fluorinated aromatic solvents, particularly trifluorotoluene (BTF) and hexafluorobenzene (BHF); tert-butyl ethers, particularly 2-ethoxy-2-methylpropane, also known as ethyl-tert-butyl-ether (ETBE); solvents comprising at least one silicon atom, particularly hexamethyldisiloxane (HMDS) and tetramethylsilane (TMS); methyl-tetrahydrofuran (MeTHF); and mixtures thereof, representing at least 50 vol.-% in relation to the total volume of the solvent system. The invention also relates to the fractions obtained using this method and to compositions containing said fractions.본 발명은 식물성 오일, 미생물 유래 오일, 또는 식물성 버터, 또는 탈취 배출물과 같은 식물성 오일 또는 미생물 유래 오일 정제 과정에서의 공업 부산물에 함유된 불검화 분획물을 추출하는 방법에 관한 것이다. 본 방법은, 최소한: A) 비누화 및 에스테르화 반응에서 선택되는 단계를 통한 상기 오일, 상기 버터 또는 식물성 오일 또는 미생물 유래 오일
来源网站:
中国工程科技知识中心
来源网址:
http://www.ckcest.cn/home/

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